2017-2018 / CHIM9245-1

Chromatographic analysis

Duration

12h Th, 8h Pr, 4h SEM

Number of credits

 Master in bioengineering : chemistry and bio-industries (120 ECTS)2 crédits 

Lecturer

Georges Lognay, Philippe Maesen

Coordinator

Eva Tyteca

Language(s) of instruction

French language

Organisation and examination

Teaching in the second semester

Units courses prerequisite and corequisite

Prerequisite or corequisite units are presented within each program

Learning unit contents

- Practical aspects of chromatography (Gas liquid chromatography and high performance liquid chromatography). - Optimisation and measurement of performances, modern instrumentation and column description. Application to the chromatographic analysis of natural molecules . - Purification procedures in organic analysis  including adsorption chromatography ; description of modern sampling methods for volatile products (VOCs): headspace techniques. Solid phase extraction (SPE) - Chiral chromatography.Multidimensionnal separations - Application of hyphenated techniques to the study of biomolecules. - Exercises : Case studies.
- Seminars

Learning outcomes of the learning unit

The applied organic chemistry course focuses on modern extraction, purification and identification methods of organic molecules from complex biological systems with special emphasize to chemical characterization, chromatographic and sampling techniques
After completing the course the student is expected to
- describe and argue about sampling and purification of the organic molecules;
- understand the different techniques (chemical analysis, derivatization, chromatography,...) for the characterization of the analytes as well as use state of the art chromatograhic methods;
- be able to discuss case studies including the theoritical aspects of the course.

Prerequisite knowledge and skills

-- CHIM9242-4 - Fundamentals of quantitative analytical chemistry
-- CHIM9238-3 - Analytical Chemistry
-- CHIM9255-3 - Organic Chemistry
-- BIOL2017-5 - Biological Chemistry
-- BIOL2019-1 - Theoretical and physical chemistry applied to structural analysis of biomolecules


--CHIM9246-A Analytical chemistry: instrumental techniques

Planned learning activities and teaching methods

Face-to-face
It is mandatory to attend all the theoritical courses and case studies

Mode of delivery (face-to-face ; distance-learning)

Lectures and case studies : 12h
Personnal work on a theme selected by the professor. It will fit the recommandations given on the BLACKBOARD plateform and will convcern the selected subject. The project has to be deposited before May, 31st 2018 at 4:00 pm

Recommended or required readings

Course notes

Assessment methods and criteria

Personal work (100%) which must be deposited asa.
Continuous evaluation, no oral examination. Course participation is mandatory

Work placement(s)

Organizational remarks

Contacts

Lognay, Georges (Em. Full Professor )   Georges.Lognay@ulg.ac.be