Duration
36h Th, 28h Pr, 10h SEM
Number of credits
Lecturer
Language(s) of instruction
French language
Organisation and examination
Teaching in the first semester, review in January
Schedule
Units courses prerequisite and corequisite
Prerequisite or corequisite units are presented within each program
Learning unit contents
- Introduction
- Drug quality control; regulatory aspects
- Drug purity and stability
- Quality control of raw materials
- Separation methods for drug analysis in complex matrix
- Quality control of end products
- Chirality and analysis
Learning outcomes of the learning unit
To provide the student the appropriate knowledge:
- to understand and use efficiently pharmacopoeias, the reference books for medicines.
to select the most appropriate analytical method for a given problem in the context of drug analysis (active substances, related substances, complex mixtures, pharmaceutical products, biological fluids).
Prerequisite knowledge and skills
- Pharmaceutical analytical chemistry - Partim I and Partim II (CHIM0320-3 and CHIM9332-1)
- Practical work - CPharmaceutical analytical chemistry - Partim I and Partim II (CHIM0321-3 and CHIM9333-1)
Planned learning activities and teaching methods
The practical work (28 h) will allow the student to gain knowledge of the monographs and the analytical approach to be integrated in order to identify and quantify drugs in complex matrix. 7 sessions will be organized.
Mode of delivery (face to face, distance learning, hybrid learning)
face-to-face, remote and SPOC
Course materials and recommended or required readings
available on ecampus
Exam(s) in session
Any session
- In-person
written exam ( multiple-choice questionnaire, open-ended questions )
Further information:
1)On-site multiple-choice written exam (MCQ) that determines eligibility for a written exam with open-ended questions. Only students who obtain a score of 10/20 or higher on the MCQ written exam are admitted to the written exam with open-ended questions.
2) On-site written exam including open-ended questions, critical thinking/problem-solving exercises, and practical laboratory-type exercises.
Final mark:
- Open-ended questions exam: 16/20
- MCQ exam: 2/20
- Practical work: 2/20
Work placement(s)
/
Organisational remarks and main changes to the course
Attendance during practical work is mandatory. In case of justified non-attendance leading to an attendance rate below 90%, the teacher reserves the right to take any action she judges necessary in order to allow the students to catch up the session(s).
Contacts
Marianne Fillet, Professor
Laboratoire d'Analyse des Médicaments, Institut de Pharmacie, CHU, Tour 4, 3ème étage, 4000 Liège
Tel : 04/3664345
e-mail : Marianne.Fillet@ulg.ac.be
Anne-Catherine Servais, Chargé de cours
Laboratoire d'Analyse des Médicaments, Département de Pharmacie, Quartier Hôpital, B36 (Tour 4), 3ème étage, 4000 Liège
acservais@uliege.be