2017-2018 / CHIM0624-1

Structure of biological macromolecules (general experimental aspects) : part a

Duration

20h Th, 10h Pr

Number of credits

 Master in bio-informatics and modelling (120 ECTS)3 crédits 

Lecturer

Paulette Charlier, Christian Damblon, Edwin De Pauw

Coordinator

Paulette Charlier

Language(s) of instruction

French language

Organisation and examination

Teaching in the first semester, review in January

Units courses prerequisite and corequisite

Prerequisite or corequisite units are presented within each program

Learning unit contents

The aim of this course is to present a series of techniques used to investigate the structure of proteins. It is divided in three parts: X-ray Crystallography, Nuclear Magnetic Resonance and Mass spectrometry. Each part is divided in theoretical and practical sections of similar importance.

I- X-ray diffraction (P. Charlier) Theoretical part: 1- Overview of the crystallographic technique, 2- Macromolecular assemblies, 3- Viral capsides and ribosomal particles structures Practical part: PYMOL tutorials for protein structures visualization and analysis.
II- Nuclear Magnetic Resonance (C. Damblon) Theoretical part: 1- Overview of the NMR technique, 2- Structure determination.
II- Mass spectrometry (E. De Pauw)

Learning outcomes of the learning unit

This course gives to the future bioinformaticians the bases necessary to understand the principles of determination of 3D protein structure by X-ray crystallography, nuclear magnetic resonance and mass spectrometry in order to enable them to make an objective use of the models. It gives them an outline of the capacities and limits of various techniques.

Prerequisite knowledge and skills

Course of physics of 1st cycle. Basic knowledge in X-ray crystallography. Good knowledge of the basic principles of the structures of proteins. Biophysical course.

Planned learning activities and teaching methods

Tutorials dedicated to the Pymol software use: obseravtion and analysis of macromolecules structures. Use of PDB database.

Mode of delivery (face-to-face ; distance-learning)

To be decided in concertation with the different lecturers.

Recommended or required readings

The PowerPoint presentations of the theoretical course will be available on CD as well as the notes of practical works. Books recommended: - "Crystallography made hook clear: With guide for users for macromolecular models." Scale Rhodos, Academic Press 2000 - "Introduction to Protein Structure" Carl Branden and John Tooze, Garland Publishing 1999 CD roms: - PS ² and Kinemage Supplement to "Introduction to Protein Structure" Carl Branden and John Tooze, Garland Publishing 1999

Assessment methods and criteria

To be decided in concertation with the different lecturers. Most probably on the basis of a research article.

Work placement(s)

Organizational remarks

Contacts

Paulette Charlier, PhD, Chargé de CoursCristallographie des macromolécules biologiques, Centre d'Ingénierie des Protéines, Département des Sciences de la Vie, Université de Liège, Institut de Physique, B5a, B-4000 Liège, Belgium Tel: +32 (0)4 366 36 19 Fax: +32 (0)4 366 49 54 E-mail : Paulette.Charlier@ulg.ac.be http://www.cip.ulg.ac.be/
DAMBLON Christian Département de chimie (sciences) / Chimie biologique structurale Bât. B6 Chimie biologique structurale allée du 6 Août 3 4000 Liège 1 Belgique Tél. ULg +32 4 3663788 Fax ULg +32 4 3664577 c.damblon@ulg.ac.be
Prof. De Pauw Edwin, Dean of Chemistry Department Mass spectrometry Laboratory CART/GIGAproteomics Liege University B4000 Liege Belgium tel direct line: +3243663415 tel secretary: +3243663414 fax: +3243663413 e.depauw@ulg.ac.be http://www.mslab.ulg.ac.be/ http://www.giga.ulg.ac.be/