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| CHIM9245-1 | Chromatographic analysis
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| Duration : | 18h Th, 6h SEM |
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| Credits/ECTS : |
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| Holder(s) : | Georges Lognay |
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| Language : | French language |
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| Course contents : | - Derivatization reaction of selected classes of analytes fot their characterization, chromatographic separation and spectrometric analysis (applications).
- Practical aspects of chromatography (Gas liquid chromatography and high performance liquid chromatography).
- Optimisation and measurement of performances, modern instrumentation and column description. Application to the chromatographic analysis of natural molecules and organic polluants.
- Extraction and purification procedures in organic analysis including adsorption chromatography ; description of modern sampling methods for volatile products analysis (hydrodistillation procedures, headspace techniques, SPME, SBSE...)
- Chiral and multidimensionnal separations
- Application of hyphenated techniques to the study of organic molecules (GC-MS, LC-MS, ...)
Case analyses. |
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| Course objective : | The applied organic chemistry course focuses on modern extraction, purification and identification methods of organic molecules from complex biological systems with special emphasize to chemical characterization, chromatographic and sampling techniques
After completing the course the student is expected to
- describe and argue about sampling and purification of the organic molecules;
- understand the different techniques (chemical analysis, derivatization, chromatography,...) for the characterization of the analytes as well as use state of the art chromatograhic methods;
- be able to discuss case studies including the theoritical aspects of the course. |
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| Prerequisites : | -- CHIM9242-2 - Fundamentals of quantitative analytical chemistry (part: 2)
-- CHIM9240-1 - Organic chemistry (first part)
-- CHIM9239-1 - Biological molecules chemistry
-- BIOL2019-1 - Theoretical and physical chemistry applied to structural analysis of biomolecules |
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| Organization : | Lectures : 18h
Seminars : 6h |
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| Written notes : | Course notes |
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| Assessment : | Oral examination (100%) |
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| Contacts : | Lognay, Georges (Professeur Ordinaire)
+32 81/62.22.20
Georges.Lognay@ulg.ac.be |
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