Analytical chemistry III - Physical methods

Physico-chemical methods of analysis

Introduction to quality assurance and quality control (QA/QC), Validation of analytical methods

Tome II: Introduction to mass spectrometry and hyphenated techniques GC-MS and LC-MS
Tome III: Spectral methods of analysis. General devices: sources of light, dispersive systems and FourierTransform systems, detectors. Emission spectrometry: flame, ICP and ICP-MS. Atomic absorption. Molecular, UV-Visible and Infra-red absorption. Raman scattering. Comparison and application of the various methods.

Electrochemical methods of analysis

Introduction to quality assurance and quality control (QA/QC), Validation of analytical methods
Tome I: Electrochemical methods of analysis. Basic Concepts; potentiometry, membrane electrodes ; electrolysis, coulometry, polarography: classical, differential and anodic stripping; amperometry.

Physico-chemical methods of analysis

To present with some details, the most current methods of analysis, based on physical processes. The aspect mainly developed is the quantitative aspect with an introduction to Quality assurance. This course however does not approach NMR, matters which belong to other courses

Electrochemical methods of analysis

To present with some details, the most current methods of analysis, based on physical processes. The aspect mainly developed is the quantitative aspect with an introduction to Quality assurance. This course however does not approach NMR, matters which belong to other courses
To present with some details, the most current methods of analysis, based on physical processes. The aspect mainly developed is the quantitative aspect with an introduction to Quality assurance. 

Physico-chemical methods of analysis

Good knowledge of the basic concepts of atomic and molecular spectroscopy.

Electrochemical methods of analysis

Good knowledge of the basic concepts of electrochemistry

Physico-chemical methods of analysis

See below<br /><br /> See below

Electrochemical methods of analysis

See below<br /><br /> See below

Physico-chemical methods of analysis

Theoretical courses (15h): 1st quadrimester. Face to face. Copies of lecture slides are available. Short movies of analytical methods have been recorded and are available on the plateform e-campus. A selection of analytical methods (polarography, GC-MS, ATR-FT-IR, Raman) are directly showed in live during the course to illustrate the theoritical concepts. 
The rehearsals  concerns certain parts of the theoretical course, illustrated by exercises. The subject covered during the rehearsals is mainly electrochemistry. Quantitative approaches by internal standard and isotope dilution are also discussed.

Electrochemical methods of analysis

Theoretical courses (15h): 1st quadrimester. Face to face. Copies of lecture slides are available. Short movies of analytical methods have been recorded and are available on the plateform e-campus. 
The rehearsals (bloc 3 Chemistry) concerns certain parts of the theoretical course, illustrated by exercises. The subject covered during the rehearsals is mainly electrochemistry. Quantitative approaches by internal standard and isotope dilution are also discussed.

Physico-chemical methods of analysis

- Full notes were written and are available for the spectral methods of analysis. They present the basic concepts which will be exposed. - Moreover, the course is presented via a powerpoint provided to the students.


- There is also a booklet of laboratory work (TPs)
There is also a booklet of exercices work (TDs)
- The students can obtain additional information, in particular in the excellent work: ANALYTICAL CHEMISTRY by SKOOG, WEST and HOLLER, DeBoeck University, 3rd edition (2015)
- Full notes including a booklet of exercices work (TDs) and aa booklet of laboratory work (TPs) are all available at the presses universitaires.

Electrochemical methods of analysis

- Full notes were written and are available for the electrochemistry part. They present the basic concepts which will be exposed. - Moreover, the course is presented via a powerpoint provided to the students.

- There is also a booklet of laboratory work (TPs)
There is also a booklet of exercices work (TDs)
- The students can obtain additional information, in particular in the excellent work: ANALYTICAL CHEMISTRY by SKOOG, WEST and HOLLER, DeBoeck University, 3rd edition (2015)
- Full notes including a booklet of exercices work (TDs) and aa booklet of laboratory work (TPs) are all available at the presses universitaires.

Physico-chemical methods of analysis

The evaluation includes:
For the bloc 3 in Chemistry 1) an exam in January : oral exam on Mass Spectrometry and Spectroscopic analytical methods (one hour of written preparation followed by an oral defense). 
The first exam session is in January, the second is in August/September
2) an examination on laboratory work (written examination in December) and an oral presentation of the method developed based on peer reviewed publication (by group of two, in December)

The distribution of the scores on the final score is as follows: -
for the exam in January: 70%  electrochemistry  (30%) and Physico-chemistry (40%) parts-
for the laboratory work (only bloc 3 in Chemistry): 30% including  the examination on practical work and the oral  presentation.
From year to year, students who graded with minimum 10/20 for their TPs do not have to repeat the practical work if their global grade is lower than 10/20.
 
For the Master 1 Engineers
4 h written exam on Mass Spectrometry and Spectroscopic analytical methods 
 

Electrochemical methods of analysis

The evaluation includes:
1) an exam in January : written part on electrochemistry (exercises + theory)
The first exam session is in January, the second is in August/September
2) an examination on laboratory work (written examination in December) and an oral presentation of the method developed based on peer reviewed publication (by group of two, in December)

The distribution of the scores on the final score is as follows: -
for the exam in January: 70%  electrochemistry (30%) and physico-chemistry (40%) parts-
for the laboratory work (only bloc 3 in Chemistry): 30% including  the examination on practical work and the oral  presentation.
From year to year, students who graded with minimum 10/20 for their TPs do not have to repeat the practical work if their global grade is lower than 10/20.

Physico-chemical methods of analysis

///

Electrochemical methods of analysis

see TP part

Travaux pratiques et répétitions

Laboratory work (65h). 
During these TDs students will have the opportunity to use electrochemical methods:
 

• The classical polarography of Pb in a Zn oxide solution
• The DPP of Cd in a Zn oxide solution;
• Amperometry of Pb from a synthetic solution;
• Anodic stripping of Pb from a white wine sample;
• Potentiometry du Ca from a synthetic solution;

Physico-chemical methods of analysis

Pr. Gauthier Eppe Institut de Chimie, Bat B6c, Local 1/9A Tel. +32-4-366.3422 e-mail. g.eppe@uliege.be
Assistant :  Gauthier Emonds-Alt (G.EmondsAlt@uliege.be)
Préparateur : Stéphane Luts
 
 

Electrochemical methods of analysis

Pr. Gauthier Eppe Institut de Chimie, Bat B6c, Local 1/9A Tel. +32-4-366.3422 e-mail. g.eppe@uliege.be
Assistant :  Gauthier Emonds-Alt (G.EmondsAlt@uliege.be)
Préparateur : Stéphane Luts
 

 

Travaux pratiques et répétitions

Pr. Gauthier Eppe Institut de Chimie, Bat B6c, Local 1/9A Tel. +32-4-366.3422 e-mail. g.eppe@ulg.ac.be
Assistants :  Gauthier Emonds-Alt : G.EmondsAlt@uliege.be
Préparateur : Stéphane Luts
 

Physico-chemical methods of analysis

The evaluation will cover the entire subject area (powerpoints +book)

Physico-chemical methods of analysis

The written exam will take place remotely via the Blackboard Collaborate and e-Campus platforms. It will consist of a series of theory questions and direct application resolutions. Its duration, still to be defined, will not exceed 4 hours.
The copy will require the student's handwritten resolution, scanned or photographed with sufficient quality, to be sent, by electrical means, before the closing time of the exam.
The exam will represent 70% of the final grade, with TP accounting for 30%. 

Physico-chemical methods of analysis

g.eppe@uliege.be