2019-2020 / CHIM9236-2

Microstructure of materials : characterization techniques

Part A

Part B

Duration

Part A : 15h Th
Part B : 10h Th

Number of credits

 Master in chemistry (120 ECTS)3 crédits 
 Master in chemistry (60 ECTS)3 crédits 

Lecturer

Part A : Catherine Henrist
Part B : Catherine Henrist

Coordinator

Catherine Henrist

Language(s) of instruction

French language

Organisation and examination

Teaching in the second semester

Schedule

Schedule online

Units courses prerequisite and corequisite

Prerequisite or corequisite units are presented within each program

Learning unit contents

Part A

This lecture consists in several lessons, each of them giving theoretical and practical information about a characteization technique aiming at the comprehensive description of materials microstructure. Among other, electron microscopies are described, as well as numerous available options like elemental analysis (EDS), crystal orientation mapping (EBSD) and electron tomography. Besides, some porosity measurements are envisaged by different techniques: X-ray tomography, gas adsorption, Archimede method, thermoporometry, ...

Learning outcomes of the learning unit

Part A

The main objective of this lecture is to give an overview of characterization techniques available to analyze the mesostructure of materials: powders, bulk, multiphased.
At the end of the lesson, the students should have gained the required scientific knowledge to properly analyze and give interpretation of a data set from each measurement technique.
They will be able to understand how the equipment works and how it can provide information about topography, chemical composition, porosity, tridimensionnal organization, or texturation of the sample.
Besides, the course aims at pushing the students to analyze a composite material based on scientific competences and critical eye, to identify how the structural charcaterization techniques can be useful, from the conception to the recycling of a material.

Prerequisite knowledge and skills

Part A

Bachelor in Sciences
basic physics of radiations, atomic structure

Planned learning activities and teaching methods

Part A

...

Mode of delivery (face-to-face ; distance-learning)

Part A

Lectures and demos stand for a total 15h ( 7 lessons)
Literature survey should be prepared at home, following a progressive scheme week-by-week ( estimated time: 10h).
The results of literature search will be shared to the classmates at the beginning of next lesson.

Recommended or required readings

Part A

copy of slides is provided

Assessment methods and criteria

Part A

Several oral presentations in front of the class, evaluation based on the quality of presentation, ability to answer questions and demonstrate comprehension of the presented data.
 

Work placement(s)

Organizational remarks

Part A

non applicable

Contacts

Part A

Catherine Henrist (catherine.henrist@ulg.ac.be)

Adaptation of teaching commitments following the COVID-19 pandemic for the May-June 2020 session

Teaching methods implemented : distance-learning

Part A

 
Experimental demos on microscopes are cancelled.
 
The lessons and literature seminars will be shared by email ( powerpoint slides).
 

Assessment subjects

Part A

 
 
no significant change

Assessment methods

Part A

 
The evaluation is based on the quaity of powerpoint presentations sent by email to the group.
 
The students also receive a feddback and have tje opportunity to answer questions.

Contacts

Part A

 
 
catherine.henrist@uliege.be

Adaptation of teaching commitments following the COVID-19 pandemic for the Aug-Sept 2020 session

Assessment subjects

Assessment methods

Contacts