Duration
25h Th
Number of credits
| Master in chemistry (120 ECTS) | 3 crédits | |||
| Master in chemistry (60 ECTS) | 3 crédits |
Lecturer
Language(s) of instruction
French language
Organisation and examination
Teaching in the first semester, review in January
Schedule
Units courses prerequisite and corequisite
Prerequisite or corequisite units are presented within each program
Learning unit contents
The course is a discovery of new technical developments in NMR and their implementation on the spectrometer.
After a lesson summarizing the theoretical and practical principles of different NMR experiments , students will be asked to select the newly published experiments ( homonuclear decoupling , Ultrafast 2D, Diffusion-DOSY ...) and to implement them onto the spectrometer . The compounds used for testing these new experiments will be chosen according to NMR experiments and can be the molecules the student will synthetized during their end-of-study work .
Learning outcomes of the learning unit
Objective 1: Acquiring the ability to record adequately all NMR experiments required for the analysis of an organic compound. Objective 2: To understand the spectral information obtained by applying a sequence of pulses. Objective 3: to choose experiences tailored to their research.
Prerequisite knowledge and skills
Course on structural analysis: CHIM-9291
Planned learning activities and teaching methods
Practical work on the NMR spectrometers 400-700 MHz. Analysis of the spectra with appropriate computer programs : TOPSPIN-MNova
Mode of delivery (face-to-face ; distance-learning)
The course schedule will be determined with the students according to the availabilities of each and the availability of the spectrometer.
Recommended or required readings
course CHIM-9291 (structural analysis)
Assessment methods and criteria
Written report on the analysis performed by the students.
Work placement(s)
Organizational remarks
Contacts
C. Damblon (C.Damblon@ulg.ac.be)