Duration
30h Th
Number of credits
| Master in chemistry (120 ECTS) | 3 crédits | |||
| Master in chemistry (60 ECTS) | 3 crédits |
Lecturer
Coordinator
Language(s) of instruction
English language
Organisation and examination
Teaching in the second semester
Schedule
Units courses prerequisite and corequisite
Prerequisite or corequisite units are presented within each program
Learning unit contents
This course presents an analysis of the transport phenomena at the basis of chemical engineering with the focus on heat and mass transfer.
- Definitions of extensive and intensive properties. Concepts of mass, momentum, and energy balance equations.
- Molecular basis for heat and mass transfer. Similarity between both.
- Energy-balance equation. Conductive and radiative contributions. Fourier's law: thermal conductivity. Stefan-Boltzmann's law: Stefan-Boltzmann constant, emissivity. Conductive stationary heat transfer: heat transfer coefficient. Conductive transient heat transfer: Fourier's number.
- Mass balances. Relative displacement flux, diffusional flux. Fick's and Maxwell-Stefan law, different molecular diffusion coefficients. Transient mass transfer. Quasi-stationary mass transfer: mass-transfer coefficient.
- Convective heat and mass transfer. Stagnant-film model, surface-renewal theory, penetration theory, two-film theory. Dimensionless numbers. Correlations of mass-transfer coefficients.
- Instabilities at interfaces induced by mass transfer.
- Dimensionless quantities
Learning outcomes of the learning unit
At the end of the course, students understand and will be able to apply theoretical concepts and the analysis methodology of transport phenomena, especially heat and mass transfer. They will be able to use these concepts to describe mathematically simple experimental systems. They will be able to use the formalism of mass and heat transfer coefficient.
Students will be able to link investigated phenomena to their mathematical representation and justify main simplifications adopted to develop the model
Prerequisite knowledge and skills
The courses "Chemistry" (CHIM0603-1), "Eléments de thermodynamique" CHIM0286-1, and "Elements of fluid mechanics" (MECA0011-2) (or courses with similar contents) should have been attended during previous years (or they should be attended the same year).
Planned learning activities and teaching methods
For chemical engineers the course is based on ex-cathedra lectures, exercises sessions, and a lab, which is realized formally as courses CHIM0022-A-c & CHIM0022-B-a. For chemists the lectures do not include the section on dimensionless quantities and the lab is not required, which is formally realized as course CHIM0022-A-c. The detailed schedule will be presented during the first lecture.
The lectures are dedicated to the detailed description of the fundamental concepts necessary for the analysis and mathematical representation of transport phenomena.
During exercise sessions students learn how to solve problems related to heat and mass-transport phenomena.
In the lab session some standard experimental methods are introduced. During laboratory sessions, students work in small teams. They have the opportunity to get familiar with experimental measurement techniques of fluid transfer properties.
Participation to laboratory sessions is mandatory for chemical engineers. The sessions have to be prepared by carefully reading the corresponding laboratory notes, which will be checked by an entrance test. If the entrance test is not passed, access to the laboratory sessions may be denied. A report, which will be graded, has to be submitted after the lab at a deadline specified in the lab notes.
Mode of delivery (face-to-face ; distance-learning)
Face-to-face
Recommended or required readings
The course material is available on the eCampus website.
Assessment methods and criteria
Participation to lab and the report are mandatory to pass the exam. At the beginning of the lab an entrance test will be condcuted to validate the ability of the student to properly handle the lab equipment.
A report of the laboratory sessions must be provided by the students within 2 weeks after these sessions. This report must present the obtained experimental results, their critical analysis, as well as answers to the questions presented in the laboratory notes. The deadline for delivering the report will also be included explicitly in the lab instructions. If the report is not received by the deadline indicated, it is graded as 0 points.
A written exam is organized during the first session in June.
The second session exam is organized in the same way as in June.
The written exam consists of exercise problems to be solved, which are similar to those presented during exercise sessions.
It is a closed-book exam. Students receive a formulary with all relevant equations.
The global grade is a weighted average of the grades obtained at the written exam (80 %) and the laboratory (including report and entrance test) (20 %).
Both exams may be oral, if the number of students is 5 or less.
Work placement(s)
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Organizational remarks
The course will be presented in English.
The course is organized during the second quadrimester.
Contacts
Andreas Pfennig PEPs - Products, Environment, and Processes Department of Chemical Engineering University of Liège Quartier Agora, Allée du six Aout 11, Bâtiment B6c, office 1/66 phone: +32 4 366-3521 e-mail: andreas.pfennig@uliege.be www.chemeng.uliege.be/Pfennig
Adaptation of teaching commitments following the COVID-19 pandemic for the May-June 2020 session
Teaching methods implemented : distance-learning
The lectures and exercises will be made available as videos, the lecture and exercise notes as pdf. The material will be available on that date, when the lecture/exercise would be delivered. The videos are available as podcast in myULiège as well as on dox. The other material will be available via eCampus and dox.
Assessment subjects
The assessment can cover all topics delivered in the course. The exam will be held as conversation, where sketches/diagrams may need to be drawn, derivations and calculations may need to be written on a sheet of paper the student should have available at the start of the exam. The lab is cancelled. The material supplied to prepare the lab will be made available and its content can be topic in the exam. There will not be any specific weight factor between questions concerning content of lecture, exercise, and lab.
Assessment methods
The exam will be oral. Otherwise modalities are unchanged. The students will need to write notes and draw sketches as well as diagrams on a sheet of paper, which will be held into the camera and photographed/scanned afterwards and supplied to the lecturer for documentation. The exam will be held as a conversation.
Contacts
e-mail: andreas.pfennig@uliege.be
Adaptation of teaching commitments following the COVID-19 pandemic for the Aug-Sept 2020 session
Assessment subjects
The assessment can cover all topics delivered in the course. The exam will be held as conversation, where sketches/diagrams may need to be drawn, derivations and calculations may need to be written on a sheet of paper the student should have available at the start of the exam. The lab is cancelled. The material supplied to prepare the lab will be made available and its content can be topic in the exam. There will not be any specific weight factor between questions concerning content of lecture, exercise, and lab.
Assessment methods
The exam will be oral. Otherwise modalities are unchanged. The students will need to write notes and draw sketches as well as diagrams on a sheet of paper, which will be held into the camera and photographed/scanned afterwards and supplied to the lecturer for documentation. The exam will be held as a conversation
Contacts
e-mail: andreas.pfennig@uliege.b