University of Liege | Version française
Academic year 2014-2015Value date : 12/05/2015
CHIM9270-1  Separation techniques in analytical chemistry

Duration :  24h Th
Number of credits :  
Master in Chemistry and Bio-industries, Professional Focus, 1st year2
Lecturer :  Stéphanie Heuskin
Language(s) of instruction :  
French language
Organisation and examination :  
Teaching in the first semester, review in January
Course contents :  
Theoretical aspects of separation techniques in analytical chemistry. Distillation - Extraction with supercritical fluid - Liquid/liquid extraction - Basic principles of the separation by column chromatography - Instrumentation and application fields of gas chromatography and of HPLC - Sampling by SPME - Sampling on solid support (SPE) - Flash chromatography. Case studies.
Learning outcomes of the course :  
The course focuses on classical and modern techniques to separate analytes in analytical chemistry.
After completing the course, the student is expected to be able to : - Describe the separation techniques which have been seen during the course. - Argue the choice of the best technique to separate various analytes from different complex matrixes. - Understand the theoretical principles of separation for each technique seen during the course. - Discuss about case studies including the theoretical aspects of the course.
Prerequisites and co-requisites/ Recommended optional programme components :  
CHIM9242-4 - Fundamentals of quantitative analytical chemistry CHIM9238-3 - Analytical chemistry CHIM9255-3 - Organic chemistry BIOL2017-5 - Biological chemistry BIOL2019-1 - Theoretical and physical chemistry applied to structural analysis of biomolecules
Planned learning activities and teaching methods :  
Face-to-face
Mode of delivery (face-to-face ; distance-learning) :  
Lectures : 20h Seminars : 4h
Recommended or required readings :  
Course notes with printed slides. Recommended book : "Chimie analytique" of Skoog, West, Holler and Crouch, 8th edition, De Boeck (2012). ISBN 978-2-8041-6295-5
Assessment methods and criteria :  
Oral examination (100%)
Work placement(s) :  
Organizational remarks :  
Contacts :  
Heuskin Stéphanie (1st assistant) +32 81 62 22 20 stephanie.heuskin@ulg.ac.be



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