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| Version 2013-2014 |
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| CHIM0220-1 | Recent nuclear magnetic resonance (NMR) methods in chemistry
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| Duration : | 15h Th |
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| Number of credits : |
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| Lecturer : | Christian Damblon |
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Language(s) of instruction :
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| French language |
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Organisation and examination :
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| Teaching in the first semester, review in January |
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Course contents :
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| The course is a practical application of NMR techniques studied in the course on Structural Analysis (CHIMI0213).
After a lesson summarizing the theoretical principles and practicalities of different NMR experiments, students will be asked to record themselves their own experiences of the compounds of their choice, for example, the compounds synthesized during their master thesis.
The proposed experiments are the following 1D 1H, 1D 13C-APT/DEPT, 2D COSY HH, HC 2D HSQC, 2D HMBC HC, 2D TOCSY HH, 2D NOESY / ROESY HH. |
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Learning outcomes of the course :
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| Objective 1: Acquiring the ability to record adequately all NMR experiments required for the analysis of an organic compound.
Objective 2: To understand the spectral information obtained by applying a sequence of pulses.
Objective 3: to choose experiences tailored to their research. |
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Prerequisites and co-requisites/ Recommended optional programme components :
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| Course on structural analysis: CHIM-0213 |
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Planned learning activities and teaching methods :
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| Practical work on the NMR spectrometer.
Analysis of the spectra with appropriate computer programs : TOPSPIN-MNova |
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Mode of delivery (face-to-face ; distance-learning) :
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| The course schedule will be determined with the students according to the availabilities of each and the availability of the spectrometer. |
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Recommended or required readings :
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| course CHIM-0213 (structural analysis) |
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Assessment methods and criteria :
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| Written report on the analysis performed by the students. |
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Work placement(s) :
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Organizational remarks :
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Contacts :
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| C. Damblon (C.Damblon@ulg.ac.be) |
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